Fatigue Threshold | Endurica LLC

Use This One Simple Trick to Ensure Rubber Part Durability

June 9, 2022August 11, 2021 by William V. Mars, Ph.D., P.E.

We’ve just added a new output to the Endurica fatigue solver: Safety Factor. This feature makes it simple to focus your analysis on whether cracks have the minimum energy required to grow. Safety Factor is a quick and inexpensive way to identity potential failure locations. It minimizes the number of assumptions you need to defend, and it is backed by hard science. You don’t need to measure or explain the many influences that together determine how fast cracks grow. You don’t need lengthy materials characterization experiments that take days or weeks. You do need to know your material’s Intrinsic Strength T₀ (ie Fatigue Threshold) and its crack precursor size c₀. The test takes about an hour using the Coesfeld Intrinsic Strength Analyser.

The Safety Factor S is computed as the ratio of T₀ to the driving force T on a potential crack precursor. If the value of the Safety Factor S = T₀/T is greater than 1, it indicates the margin by which crack growth is avoided. If S is less than 1, it indicates that crack growth is inevitable. The calculation of the Safety Factor includes a search for the most critical plane, as we do for our full fatigue life computations.

Although the Safety Factor can’t tell you how long a part will endure, it nevertheless does offer great utility. You can make a contour plot showing the locations in your part where the Safety Factor is the lowest. This is a quick and inexpensive way to identity potential failure locations. You can make statements about the reserve capacity of your design that are easy to communicate and understand with a wide audience.

A vibration isolation grommet operating under small displacement

A vibration isolation grommet operating under large displacement

The images above show a vibration isolation grommet operating under small (Safety Factor 2.6) and large displacements (Safety Factor 0.83). Color contours indicate the Endurica-computed Safety Factor, and use the same scale for both images. Large Safety Factors are shown in blue. Safety Factors approaching 1 are shown in red. Safety Factors smaller than 1 are indicated in black. These results show that the grommet can be expected to operate indefinitely under the small displacements, but that large displacements will produce cracks at some point, in the regions colored black.

Durability by Design on Any Budget

June 9, 2022June 7, 2021 by William V. Mars, Ph.D., P.E.

So, you’ve got a tricky durability problem to solve, a budget, and a deadline. Let’s look at a helpful framework for sorting which Endurica workflows you need. In the grid below, each row represents a potential approach you can take. The approaches are, in order of increasing complexity and cost, the Infinite Life approach, the Safe Life approach, the Damage Tolerant approach, and the Fail Safe approach.

The Infinite Life approach is by far the simplest approach. Here, we say that damage will not be allowed at all. All locations in the part must operate, at all times, below the fatigue limit (ie intrinsic strength) of the rubber. The required material testing is minimal: we need only know the fatigue limit T₀ and the crack precursor size c₀. We avoid the question of how long the part may last, and we focus on whether or not we can expect indefinite life. We report a safety factor S indicating the relative margin (ie S = T₀ / T) by which each potential failure location avoids crack development. When S>1, we predict infinite life. For S<=1, failure occurs in finite time and we must then go on to the next approach…

In the Safe Life approach, the chief concern is whether or not the part’s estimated finite life is adequate relative to the target life. The material characterization now becomes more sophisticated. We must quantify the various “special effects” that govern the crack growth rate law (strain crystallization, temperature, frequency, etc.). We consider the specific load case(s), then compute and report the number of repeats that the part can endure. If the estimated worst-case life is greater than the target life then we may say that the design is safe under the assumptions considered. If not, then we may need to increase the part’s load capacity, or alternatively to decrease the applied loading to a safe level. In critical situations, we may also consider implementing the next level…

The Damage Tolerant approach acknowledges that, whatever the reasons for damage, the risk of failure always exists and therefore should be actively monitored. This approach monitors damage development via inspection and via tracking of accrued damage under actual loading history. A standard nominal load case may be assumed for the purpose of computing a remaining residual life, given the actual loading history to date. Changes in material properties due to cyclic softening or ageing may also be tracked and considered in computing forecasts of remaining life.

The Fail Safe approach takes for granted that failure is going to occur, and obliges the designer to implement measures that allow for this to happen safely. This can take the form of a secondary / redundant load path that carries the load once the primary load path has failed. It can take the form of a sacrificial weak link / “mechanical fuse” that prevents operation beyond safe limits. It can take the form of a Digital Twin that monitors structural health, senses damage, and requests maintenance when critical damage occurs.

The last three columns of the grid show which Endurica fatigue solver workflows align with each design approach. The Endurica solvers give you complete coverage of all approaches. Whether you need a quick Infinite Life analysis of safety factors for a simple part, or deep analysis of Damage Tolerance or Fail Safety, or anything in-between, our solvers have just what you need to get durability right.

Durability Insights from the ISA for Tire Tread Compound Development

June 9, 2022June 11, 2020 by Christopher G. Robertson, Ph.D.

My last blog post (Getting a Quick Read on Durability with the Intrinsic Strength Analyser) highlighted a one-hour test on the Intrinsic Strength Analyser (ISA) to screen elastomer materials for long-term fatigue performance, with applications in materials R&D and plant mixing quality control. To illustrate the use of this approach for rubber compound development, we recently had the opportunity to collaborate with Dr. Nihat Isitman from Goodyear Tire & Rubber Company in Akron, Ohio and Dr. Radek Stoček from Polymer Research Laboratory in Zlín, Czech Republic.¹ Dr. Isitman led this project and was scheduled to present our research at the Spring 2020 Technical Meeting of the ACS Rubber Division, but the meeting was cancelled due to COVID-19 precautions. Instead, the Rubber Division is offering the content online, and the meeting presentations are available here for a modest fee.

Our study considered model tread compounds based on the well-known green tire formulation, which is a compatible blend of solution styrene-butadiene rubber (SBR) and high-cis butadiene rubber (BR) that is reinforced with a silica-silane system for low rolling resistance (improved fuel economy) passenger tires. Additional production compounds used in actual tire treads were also tested, but the proprietary results for these materials were not included in the public presentation. The SBR/BR ratio, silica loading, and crosslink density were all varied in this investigation. For each rubber formulation, the ISA was used to measure the fatigue threshold (T₀) and critical tearing energy (tear strength; T_c), which bracket the two ends of the fatigue crack growth curve as shown below.

The established cutting method of Lake and Yeoh^2,3is used for assessing T₀ on the ISA, and the one-hour test on this benchtop instrument is concluded with a tearing procedure to measure T_c. The ISA is manufactured by Coesfeld GmbH & Co. in Dortmund, Germany, and distributed in the Americas by Endurica LLC (see photo).

The slide image below summarizes the key findings of this research collaboration. Optimization of T₀ and T_c is possible thanks to different sensitivities to the various compounding variables. It is important to measure both fatigue threshold and tear strength to quantify durability potential of rubber materials, and the ISA is an efficient and effective instrument for these measurements. To learn more about this testing equipment for the rubber lab, please visit our Instruments page and contact us at info@endurica.com with questions.

References

N. Isitman, R. Stoček, and C. G. Robertson, “Influences of compounding attributes on intrinsic strength and tearing behavior of model tread rubber compounds”, paper scheduled to be presented at the 197^th Technical Meeting of the Rubber Division, ACS, Independence, OH, April 28-30, 2020 (online presentation due to meeting cancellation).
G. J. Lake and O. H. Yeoh, “Measurement of Rubber Cutting Resistance in the Absence of Friction”, International Journal of Fracture 14, 509 (1978).
C. G. Robertson, R. Stoček, C. Kipscholl, and W. V. Mars, “Characterizing the Intrinsic Strength (Fatigue Threshold) of Natural Rubber/Butadiene Rubber Blends”, Tire Sci. Technol. 47, 292 (2019).

Getting a Quick Read on Durability with the Intrinsic Strength Analyser

June 9, 2022March 27, 2020 by Christopher G. Robertson, Ph.D.

There is now a one-hour test on a benchtop instrument for the rubber lab to screen materials for long-term fatigue performance. Please continue reading to learn more about this commercialization of a classical elastomer characterization methodology.

Rubber products manufacturers and raw materials suppliers seeking improved materials for next-generation applications depend on lab tests to predict end-use performance. These predictive tests should balance accuracy, relevance, and testing time. The testing time component is particularly challenging when the performance characteristic of interest is fatigue lifetime. The image of traditional fatigue testers chattering along for days or weeks comes to mind for those of us with experience in industrial rubber labs. The time consideration is the reason why tensile stress-strain testing (stretching a material to high strains until failure) is the most common physical test for the fracture behavior of rubber, in clear contrast to the most prevalent application condition for rubber products which is cyclic loading (fatigue) at much lower strains.

Fatigue crack growth is a key element of elastomer behavior that must be determined in order to predict durability, as illustrated below. For example, fatigue crack growth (FCG) testing provides the FCG rate law that is essential for predicting when and where cracks will show up in rubber products using Endurica’s elastomer fatigue software for finite element analysis [https://endurica.com/integrated-durability-solutions-for-elastomers/]. Endurica has developed a finitely scoped, reduced variability measurement approach¹ which is used in our Fatigue Property Mapping testing services and is available on the Coesfeld Tear and Fatigue Analyser (TFA). Our standard FCG measurement protocol takes 20 hours of continuous testing. This testing time is very efficient for characterizing best candidate materials in the development process, but a faster test is needed for narrowing down, for example, 20 initial materials to 5 best candidates or for use in a plant lab to monitor quality of rubber compounding processes.

Key Components of Elastomer Fatigue and Failure

The Intrinsic Strength Analyser (ISA) is a recent addition to the durability testing solutions for elastomers. The ISA was developed through a partnership between Coesfeld GmbH & Co. (Dortmund, Germany) and Endurica LLC (Findlay, OH, USA), and this benchtop instrument employs a testing protocol based on the long-established cutting method of Lake and Yeoh.^3,4 Endurica’s president, Dr. Will Mars, discusses the importance of measuring intrinsic strength (fatigue threshold) in this video on our YouTube channel which also shows some footage of the ISA in operation:

https://www.youtube.com/watch?v=BL92ppsJZfE

The fatigue crack growth curve of rubbery materials is bounded by the fatigue threshold, T₀, on the low tearing energy (T) side and by the critical tearing energy (tear strength), T_c, at the high-T end. This is depicted in the generalized figure below. A streamlined one-hour procedure on the ISA can measure both T₀ and T_c which can then be used to estimate the slope (F) of the intermediate FCG power law response that correlates well with the actual F from rigorous FCG testing using the TFA (see figure). More information about this quick ISA approach to characterizing rubber crack growth behavior for materials development and quality control can be found in the Annual Review 2019 issue of Tire Technology International (open access).²

ISA graph showing Crack Growth Rate compared to tearing energy

The fatigue crack growth slope

The fatigue crack growth slope, F, from the ISA should be considered an approximate value that is useful for comparing the relative FCG behavior of materials. However, the determination of T₀ on the ISA is highly quantitative and the only realistic option for assessing this parameter, since the near-threshold crack growth testing on the TFA needed to define T₀ would take about a month. The implementation areas for the ISA and TFA are compared in the following table. A very conservative approach to product development for elastomer durability is to create a combination of material behavior and component design that places the final operation of the rubber product below the fatigue threshold. If this is your company’s approach to engineering for durability, then the ISA is the testing instrument you need.

Durability Testing Solutions for the Rubber Lab

Crack precursor size is another key characteristic of elastomers that needs to be quantified in order to predict durability. In combination with a standard tensile stress-strain test, the critical tearing energy (T_c) from the ISA can also be used to assess crack precursor size, as we showed recently in an open access publication.⁵

Endurica is the exclusive Americas distributor of the Coesfeld ISA and TFA instruments. Endurica’s efficient and effective testing protocols are provided on these high-quality instruments for the rubber laboratory. To learn more about how to add these testing capabilities to your lab, please contact us at info@endurica.com.

References

J. R. Goossens and W. V. Mars, “Finitely Scoped, High Reliability Fatigue Crack Growth Measurements”, Rubber Chem. Technol. 91, 644 (2018).
C. G. Robertson, R. Stoček, R. Kipscholl, and W. V. Mars, “Characterizing Durability of Rubber for Tires”, Tire Technology International, Annual Review 2019, pp. 78-82.
G. J. Lake and O. H. Yeoh, “Measurement of Rubber Cutting Resistance in the Absence of Friction”, International Journal of Fracture 14, 509 (1978).
C. G. Robertson, R. Stoček, C. Kipscholl, and W. V. Mars, “Characterizing the Intrinsic Strength (Fatigue Threshold) of Natural Rubber/Butadiene Rubber Blends”, Tire Sci. Technol. 47, 292 (2019).
C. G. Robertson, L. B. Tunnicliffe, L. Maciag, M. A. Bauman, K. Miller, C. R. Herd, and W. V. Mars, “Characterizing Distributions of Tensile Strength and Crack Precursor Size to Evaluate Filler Dispersion Effects and Reliability of Rubber”, Polymers 12, 203 (2020).