Validation

“Is it validated?” – that’s often the first question we hear after introducing our durability simulation capabilities. And for good reason, given the weight that hangs on the hinge of product durability. Endurica takes verification and validation (V&V) very seriously. Let’s look at what that means.

First, it means that our tools are built on well-known, well-established foundations.  These foundations include 1) definition of material / crack behavior via fracture mechanics (Rivlin and Thomas, 1953), 2) integration of the crack growth rate law to predict fatigue life (Gent, Lindley and Thomas, 1964), 3) the fact that crack precursors occur naturally in all locations and all orientations in a rubber sample (Choi and Roland 1996, Huneau et al 2016), 4) hyperelastic stress-strain laws compatible with commercial FEA codes (see Muhr 2005 for an excellent review), and 5) rubber’s fatigue threshold (Lake and Thomas 1967).  The validation case thus begins with the cumulative authority of thousands of reports that have confirmed these classical results over nearly 70 years.

Critical plane analysis for rubber has now been around for 20+ years, and it has been validated in multiple ways (material level, component level, system level), across multiple experimental programs (industrial and academic), by multiple independent research groups working on multiple applications (see Google/scholar, for example).  It has been validated that: 1) it correctly predicts crack plane orientation under uniaxial, proportional and nonproportional loadings (Harbour et al 2008), 2) it correctly predicts fatigue life across different modes of deformation (Mars 2002), 3) it correctly accounts for the effects of crack closure (Mars 2002), 4) it correctly predicts the development of off-axis cracks for nonrelaxing cycles in strain-crystallizing materials (Ramachandran 2017), 5) it correctly predicts the effects of finite straining on crack orientation (Mars and Fatemi 2006).

The literature is full of old experiments that we have used as validation targets.  We have validated Endurica’s strain crystallization models by simulating experimental results published by Cadwell et al (1940) and by Fielding et al (1943).  We have validated the ability to predict deformation mode effects by simulating experimental results for simple and biaxial tension published by Roberts and Benzies (1977).  We have validated Endurica’s temperature dependence against measurements reported by Lake and Lindley (1964).  We have validated against multiaxial fatigue experiments reported by Saintier, Cailletaud and Piques (2006).

We’ve done our own validation experiments.  My PhD dissertation (University of Toledo, 2001) contains an extensive database of tension/torsion/compression fatigue tests against which our critical plane algorithms were validated.  Two additional PhD dissertations that I co-advised generated additional validations.  Dr. Malik Ait Bachir’s thesis (2010) validated mathematically that the scaling law we use for small cracks is valid across all multiaxial loading states.  Dr. Ryan Harbour’s thesis (2006) contains a database of multiaxial, variable amplitude fatigue experiments against which our rainflow and damage accumulation procedures were extensively validated.

Validation from partners.  We partner with several testing labs.  We have invested in testing protocols that produce clean, accurate data and we have run validation programs with our partners to verify the effectiveness of our testing protocols.  We’ve demonstrated significant improvements to test efficiency and reproducibility (Goosens and Mars 2018) and (Mars and Isasi 2019).  We’ve validated techniques for estimating precursor size and size distribution (Robertson et al 2020, Li et al 2015).

Validation from users.  Three (3) of the top 12 tire companies and six (6) of the top 10 global non-tire rubber companies now use our solutions.  Most of our users have run internal validation programs to show the effectiveness of our solutions for their applications.  Most of these studies are unpublished, but the fact that our user base has continued growing at ~20%/year for 12 years (as of this year) says something important both about the technical validation case and the business validation case.  Validation studies have been published with the US Army (Mars, Castanier, Ostberg 2017), GM (Barbash and Mars 2016), Tenneco (Goossens et al 2017) and Caterpillar (Ramachandran et al 2017).

Validation from external groups.  There are several academic groups that have independently applied and validated components of our approach.  There are too many to list completely, but a few recent examples include Zarrin-Ghalami et al (2020), Belkhira et al (2020) and Tobajas et al (2020).

Software verification, benchmarking and unit testing.  In addition to the experimental validations mentioned above, each time we build a new version of our software, we execute a series of automated tests.  These tests verify every line of code against expected function, and they ensure that as we add new features, we do not introduce unintended changes.  The benchmarks include tests that verify things like coordinate frame objectivity (rigid rotations under static load should do no damage and the same strain history written in two different coordinate systems should have the same life), and check known results pertaining to material models and cycle counting rules.  You can read more about our software quality processes here.

It is safe to say that no other solution for fatigue life prediction of rubber has been tested and validated against a larger number of applications than Endurica’s.

References

Aıt-Bachir, M. “Prediction of crack initiation in elastomers in the framework of Configurational Mechanics.” PhD diss., Ph. D. thesis, Ecole Centrale de Nantes, Nantes (France), 2010.

Barbash, Kevin P., and William V. Mars. Critical plane analysis of rubber bushing durability under road loads. No. 2016-01-0393. SAE Technical Paper, 2016.

Belkhiria, Salma, Adel Hamdi, and Raouf Fathallah. “Cracking energy density for rubber materials: Computation and implementation in multiaxial fatigue design.” Polymer Engineering & Science (2020).

Cadwell, S. M., R. A. Merrill, C. M. Sloman, and F. L. Yost. “Dynamic fatigue life of rubber.” Rubber Chemistry and Technology 13, no. 2 (1940): 304-315.

Choi, I. S., and C. M. Roland. “Intrinsic defects and the failure properties of cis-1, 4-polyisoprenes.” Rubber chemistry and technology 69, no. 4 (1996): 591-599.

Fielding, J. H. “Flex life and crystallization of synthetic rubber.” Industrial & Engineering Chemistry 35, no. 12 (1943): 1259-1261.

Goossens, J.R., Mars, W., Smith, G., Heil, P., Braddock, S. and Pilarski, J., 2017. Durability Analysis of 3-Axis Input to Elastomeric Front Lower Control Arm Vertical Ride Bushing (No. 2017-01-1857). SAE Technical Paper. https://doi.org/10.4271/2017-01-1857

Goossens, Joshua R., and William V. Mars. “Finitely Scoped, High Reliability Fatigue Crack Growth Measurements.” Rubber Chemistry and Technology 91, no. 4 (2018): 644-650. https://doi.org/10.5254/rct.18.81532

Harbour, Ryan Joseph. Multiaxial deformation and fatigue of rubber under variable amplitude loading. Vol. 67, no. 12. 2006.

Harbour, Ryan J., Ali Fatemi, and Will V. Mars. “Fatigue crack orientation in NR and SBR under variable amplitude and multiaxial loading conditions.” Journal of materials science 43, no. 6 (2008): 1783-1794.

Huneau, Bertrand, Isaure Masquelier, Yann Marco, Vincent Le Saux, Simon Noizet, Clémentine Schiel, and Pierre Charrier. “Fatigue crack initiation in a carbon black–filled natural rubber.” Rubber Chemistry and Technology 89, no. 1 (2016): 126-141.

Lake, G. J., and P. B. Lindley. “Cut growth and fatigue of rubbers. II. Experiments on a noncrystallizing rubber.” Journal of Applied Polymer Science 8, no. 2 (1964): 707-721.

Li, Fanzhu, Jinpeng Liu, W. V. Mars, Tung W. Chan, Yonglai Lu, Haibo Yang, and Liqun Zhang. “Crack precursor size for natural rubber inferred from relaxing and non-relaxing fatigue experiments.” International Journal of Fatigue 80 (2015): 50-57.

Mars, William Vernon. Multiaxial fatigue of rubber. 2001.

Mars, Will V. “Cracking energy density as a predictor of fatigue life under multiaxial conditions.” Rubber chemistry and technology 75, no. 1 (2002): 1-17.

Mars, W. V., and A. Fatemi. “Analysis of fatigue life under complex loading: Revisiting Cadwell, Merrill, Sloman, and Yost.” Rubber chemistry and technology 79, no. 4 (2006): 589-601.

Mars, W. V., and A. Fatemi. “Nucleation and growth of small fatigue cracks in filled natural rubber under multiaxial loading.” Journal of materials science 41, no. 22 (2006): 7324-7332.

Mars, W. V. “Computed dependence of rubber’s fatigue behavior on strain crystallization.” Rubber Chemistry and Technology 82, no. 1 (2009): 51-61. https://doi.org/10.5254/1.3557006

Mars, William V., Matthew Castanier, David Ostberg, and William Bradford. “Digital Twin for Tank Track Elastomers: Predicting Self-Heating and Durability.” In Proceedings of the 2017 Ground Vehicle Systems Engineering and Technology Symposium (GVSETS). 2017.pdf here

Mars, W. V., and M. Isasi. “Finitely scoped procedure for generating fully relaxing strain-life curves.” In Constitutive Models for Rubber XI: Proceedings of the 11th European Conference on Constitutive Models for Rubber (ECCMR 2019), June 25-27, 2019, Nantes, France, p. 435. CRC Press, 2019.

Muhr, A. H. “Modeling the stress-strain behavior of rubber.” Rubber chemistry and technology 78, no. 3 (2005): 391-425.Lake and Thomas 1967

Ramachandran, Anantharaman, Ross P. Wietharn, Sunil I. Mathew, W. V. Mars, and M. A. Bauman. “Critical Plane Selection Under Nonrelaxing Simple Tension with Strain Crystallization.” In Fall 192nd Technical Meeting of the Rubber Division, pp. 10-12. 2017.

Rivlin, R. S., and A. G. Thomas. “Rupture of rubber. I. Characteristic energy for tearing.” Journal of polymer science 10, no. 3 (1953): 291-318.Gent, Lindley and Thomas, 1964

Roberts, B. J., and J. B. Benzies. “The relationship between uniaxial and equibiaxial fatigue in gum and carbon black filled vulcanizates.” Proceedings of rubbercon 77, no. 2 (1977): 1-13.

Robertson, Christopher G., Lewis B. Tunnicliffe, Lawrence Maciag, Mark A. Bauman, Kurt Miller, Charles R. Herd, and William V. Mars. “Characterizing Distributions of Tensile Strength and Crack Precursor Size to Evaluate Filler Dispersion Effects and Reliability of Rubber.” Polymers 12, no. 1 (2020): 203. Pdf here

Saintier, Nicolas, Georges Cailletaud, and Roland Piques. “Multiaxial fatigue life prediction for a natural rubber.” International Journal of Fatigue 28, no. 5-6 (2006): 530-539.

Tobajas, Rafael, Daniel Elduque, Elena Ibarz, Carlos Javierre, and Luis Gracia. “A New Multiparameter Model for Multiaxial Fatigue Life Prediction of Rubber Materials.” Polymers 12, no. 5 (2020): 1194.

Zarrin-Ghalami, Touhid, Sandip Datta, Robert Bodombo Keinti, and Ravish Chandrashekar. Elastomeric Component Fatigue Analysis: Rubber Fatigue Prediction and Correlation Comparing Crack Initiation and Crack Growth Methodologies. No. 2020-01-0193. SAE Technical Paper, 2020.